One of my fellow chemists asked me if I knew where she could purchase a single
silver iodide crystal, and after a while searching without an answer I looked up the synthesis of this metal compound. The procedure is fairly simple starting with dissolving
silver nitrate (AgNO
3) in water, followed with the addition of
potassium iodide (KI). A yellow precipitate will form immediately containing both the α-AgI and the β-AgI crystals which can be separated through different dissolution methods.
AgNO
3 (aq) + KI
(aq) → KNO
3 (aq) + AgI
(s)
Source: O. Glemser, H. Saur "Silver Iodide" in Handbook of Preparative Inorganic Chemistry, 2nd Ed. Edited by G. Brauer, Academic Press, 1963, NY. Vol. 1. p. 1036-7
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